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- W2020133093 abstract "A mass fragmentographic method for determination of 4-methylpyrazol in serum is described. 4-Methylpyrazol with three atoms of deuterium in the methyl group is added to a fixed amount of serum as internal standard. After extraction of the serum with ether, the amount of unlabeled 4-methylpyrazol is determined from the ratio between the recordings at me 82 and me 85 obtained after analysis with a combined gas chromatograph—mass spectrometer equipped with a MID-unit (multiple ion detector). With this method 4-methylpyrazol could be determined in concentrations down to about 0.1 μg/ml corresponding to about 1 μM. The relative standard deviation of the method in the range 4–21 μM was less than 2%. The method could be used for determination of disappearance rate of 4-methylpyrazol in experimental animals as well as humans." @default.
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- W2020133093 date "1975-03-01" @default.
- W2020133093 modified "2023-10-14" @default.
- W2020133093 title "Determination of 4-methylpyrazol in serum with mass fragmentography" @default.
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- W2020133093 doi "https://doi.org/10.1016/0006-2944(75)90122-2" @default.
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