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- W2020140318 abstract "The β-diketone complexes of vanadium(IV), VO(dik)2 (where dik ≡; btfac, tfac, ttfac, acac, bzac and bzbz) have been prepared either by the reaction of vanadium pentoxide with the appropriate ligand in toluene under reflux for 24 h or by the reaction of a warm aqueous or ethanolic solution of vanadium sulphate with the ligand. The oxovanadium(IV) complexes react with sulphur oxide dichloride and dibromide and phosphorus pentachloride to form dihalovanadium(IV) diketonate complexes. These compounds have been characterized by elemental analysis, melting point measurements, IR and Raman spectra, magnetic susceptibility measurements, electron spin resonance (ESR) and mass spectral studies and X-ray powder diffraction." @default.
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- W2020140318 date "1987-02-01" @default.
- W2020140318 modified "2023-10-18" @default.
- W2020140318 title "Preparation, characterization and reactions of vanadium(IV) β-diketonate complexes" @default.
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- W2020140318 doi "https://doi.org/10.1016/0022-5088(87)90216-5" @default.
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