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- W2020164345 abstract "A new hydrogen terminated 2,2′-bidipyrrin ligand was prepared from a bipyrrole dialdehyde and 3,4-diethylpyrrole by a POCl3 induced condensation and isolated as the nickel(II) chelate. Unexpectedly a side reaction occured when base-deficient and aerobic conditions were chosen in the metalation step. This side reaction led to a novel pentapyrrolic nickel(II) complex with one externally bound pyrrole ring. Further studies showed that the reactions of 2,2′-bidipyrrins with 3,4-diethyl- or 2,3,4-trimethylpyrrole and an oxidant resulted in a stepwise exchange of the terminal pyrrole moieties and, in the former case, the introduction of one additional pyrrole ring into one of the two meso positions of the open-chain tetrapyrrole." @default.
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- W2020164345 date "2007-02-01" @default.
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- W2020164345 title "Oxidative Pyrrole Exchange andmeso Pyrrylation – Unexpected Reactions of Open-Chain Tetrapyrrolic 2,2′-Bidipyrrins" @default.
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- W2020164345 doi "https://doi.org/10.1002/zaac.200600268" @default.
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