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- W2020176608 abstract "An economic and practical method for preparing enantiomerically pure [1,1′-binaphthalene]-2,2′-diols is reported. Thus, a condensate of threo-(1S,2S)-2-amino-1-(4-nitrophenyl)propane-1,3-diol and cyclohexanone (CHANP) was used as a resolving agent. A 2 : 1 : 1 mixture of racemic [1,1′-binaphthalene]-2,2′-diol, boric acid, and CHANP was refluxed for several hours in THF or MeCN to give a white precipitate of bis{(R)-[1,1′-binaphthalene]-2,2′-diol}boric acid CHANP derivative, from the precipitate, and a filtrate separated from the precipitate, (R)- and (S)-[1,1′-binaphthalene]-2,2′-diol of 100% ee were obtained in ca. 65% yield, respectively." @default.
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- W2020176608 date "2003-01-01" @default.
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- W2020176608 title "A New and Practical Method for Preparing Enantiomerically Pure [1,1′-Binaphthalene]-2,2′-diol: Resolution of Racemic [1,1′-Binaphthalene]-2,2′-diol withthreo-(1S,2S)-2-Amino-1-(4-nitrophenyl)propane-1,3-diolCyclohexanone Condensate" @default.
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