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- W2020178423 abstract "The action of P2O5 in DMSO on methyl α-d-glucopyranoside, sucrose and trehalose afforded nondializable, phosphorylated glycans in 6~34% yields. Polysucrose has a molecular weight of ~9,500. The synthetic glycans consist of carbohydrate (46~59%) and P (11.4~13.1%) and show reducing sugar values (5.0~30.8%). The alkaline hydrolysis of polysucrose was accompanied with a depolymerization and afforded sugar phosphates and oligosaccharides. The periodate oxidation gave formic acid (0.15~0.34 mole) and formaldehyde (0.07~0.17 mole/monosaccharide residue). The methylation study indicated their variously branched structures. 2,3,4,6-Tetra-O-methyl-d-glucose was found in only 0.7 ~3.2% yields, and this is in agreement with their weak precipitation reactions with Con A. It is considered that the glycans are produced from nonreducing mono- and oligosaccharides by dehydration, transglycosidation and esterification with phosphate." @default.
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- W2020178423 date "1975-01-01" @default.
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- W2020178423 title "Phosphorylated glycans produced from nonreducing mono- and oligosaccharides by the action of P2O5 in dimethyl sulfoxide, and their interactions with concanavalin A." @default.
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- W2020178423 doi "https://doi.org/10.1271/bbb1961.39.1963" @default.
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