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- W2020194347 abstract "Abstract Chloromethylene iminium salts (Vilsmeier reagents) have a long history and thoroughly investigated chemistry(1). Chloro-N, N-dimethylforminium chloride 1 is most conveniently generated by the reaction of N, N-dimethylformamide (DMF) with oxalyl chloride(2). The reagent has also been obtained usingthicnyl chloride at elevated temperature and a variety of acid chlorides(1b). The literature describes several examples of the use of thionyl chloride in combination with DMF in which 1 or a related species is thought to function as the reactive intermediate in the transformation of amides to nitriles(3)." @default.
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- W2020194347 date "1980-01-01" @default.
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- W2020194347 title "A Rapid and Efficient Method for Dehydration of Primary Amides to Nitriles. Preparation of Acrylonitrile Derivatives" @default.
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- W2020194347 doi "https://doi.org/10.1080/00397918008064272" @default.
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