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• W2020273722 abstract "A new dinuclear iron nitrosyl complex [Fe 2 (C 14 H 12 N 3 S) 2 (NO) 4 ] ( 1 ) (C 14 H 12 N 3 S = 2-mercapto-1-[2-(4-pyridyl)-ethyl]-benzimidazolyl) has been obtained by the reaction of Fe(NO) 2 (CO) 2 with 2-mercapto-1-[2-(4-pyridyl)-ethyl]-benzimidazole in CH 3 OH under moderate condition. Complex 1 was characterized by IR, UV–vis, electrochemistry and single crystal X-ray diffraction. IR spectrum displays two strong characteristic NO stretching frequencies ( ν NO ) in solution and in solid state. Cyclic voltammetry shows one irreversible, two quasi-reversible and two reversible one-electron reductions and irreversible oxidizations. This result is consistent with the fact that complex 1 is very unstable and ready to lose NO in the air. As showing in the single crystal X-ray diffraction, complex 1 forms a “chair-shape” structure by the connections of two iron centers and S–C–N frames of benzimidazole. The dihedral angle of benzimidazole ring and 2Fe–2S plane is 73.6°. The crystal data are the following: 1, monoclinic, space group P 2(1)/ c , a = 10.43940(10) Å, b = 16.0900(2) Å, c = 10.13240(10) Å, α = 90°, β = 111.0940(10)°, γ = 90°, V = 1587.89(3) Å 3 , Z = 4." @default.
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• W2020273722 date "2009-04-01" @default.
• W2020273722 modified "2023-10-16" @default.
• W2020273722 title "Synthesis, characterization and crystal structure of a dinuclear iron nitrosyl complex with 2-mercapto-1-[2-(4-pyridyl)-ethyl]-benzimidazolyl" @default.
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• W2020273722 doi "https://doi.org/10.1016/j.molstruc.2009.02.010" @default.
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