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- W2020343482 abstract "Abstract We analyze the influence of the preparation method and Re content on the chemical stability, thermodynamic properties and superconducting response of Hg 1−x Re x Ba 2 CuO 4+δ (0 samples. The route of synthesis is also investigated to optimize the incorporation of Re in the Hg-1201 structure. The samples are characterized by X-ray diffraction, scanning electron microscopy and microanalysis, and the influence of Re content on the oxygen stoichiometry is studied by means of thermogravimetry. The superconducting response of samples and their aging are studied by d.c. susceptibility. We find that Re doping increases the thermodynamic stability due to the incorporation of highly bonded oxygen atoms in the (Hg,Re)–Oδ planes. In addition, Re-free samples prepared with Hg excess remain stable for long periods under ambient atmosphere. An optimal synthesis method and the Hg excess would avoid the formation of amorphous phases composed of Ba and Cu oxides which are responsible of such degradation in samples with Hg deficiency." @default.
- W2020343482 created "2016-06-24" @default.
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- W2020343482 date "2001-01-01" @default.
- W2020343482 modified "2023-09-30" @default.
- W2020343482 title "Synthesis methods and characterization of (Hg,Re)-1201" @default.
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- W2020343482 doi "https://doi.org/10.1016/s0921-4534(00)01545-8" @default.
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