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• W2020456487 abstract "A mechanistic study of the hydroselenation of alkynes catalyzed by Pd(PPh3)4 and Pt(PPh3)4 has shown that the palladium complex gives products of both SeH and SeSe bond addition to the triple bond of alkynes, while the platinum complex selectively catalyzes SeH bond addition. The key intermediate of PhSeH addition to the metal center, namely Pt(H)(SePh)(PPh3)2, was detected by 1H-NMR spectroscopy. The analogous palladium complex rapidly decomposes with evolution of molecular hydrogen. A convenient method was developed for the preparation of Markovnikov hydroselenation products H2CC(SePh)R, and the scope of this reaction was investigated. The first X-ray structure of the Markovnikov product H2CC(SePh)CH2N+HMe2·HOOCCOO− is reported." @default.
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• W2020456487 date "2003-08-01" @default.
• W2020456487 modified "2023-10-12" @default.
• W2020456487 title "Palladium and platinum catalyzed hydroselenation of alkynes: SeH vs SeSe addition to CC bond" @default.
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• W2020456487 doi "https://doi.org/10.1016/s0022-328x(03)00546-1" @default.
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