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- W2020537072 abstract "The dioxopiperazine metabolites of quinapril in plasma and urine were extracted with hexane-dichloroethane (1:1) under acidic conditions. Following derivatization with pentafluorobenzyl bromide and purification of the desired reaction products using a column packed with silica gel, the metabolites were analysed separately by capillary column gas chromatography-electron-impact mass spectrometry with selected-ion monitoring. The limits of quantitation for the metabolites were 0.2 ng/ml in plasma and 1 ng/ml in urine. The limits of detection were 0.1 ng/ml in plasma and 0.5 ng/ml in urine, at a single-to-noise ratio of greater than 3 and greater than 5, respectively. The proposed method is applicable to pharmacokinetic studies." @default.
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- W2020537072 date "1992-07-01" @default.
- W2020537072 modified "2023-09-25" @default.
- W2020537072 title "Determination of dioxopiperazine metabolites of quinapril in biological fluids by gas chromatography—mass spectrometry" @default.
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- W2020537072 doi "https://doi.org/10.1016/0378-4347(92)80417-o" @default.
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