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- W2020553631 abstract "Abstract Ethylidene diacetate was prepared by reacting dimethyl ether, acetic acid and syngas in the presence of a catalytic system comprising RhI 3 , PPh 3 and CH 3 I. The effects of reaction temperature, pressure, time and the CO/H 2 molar ratio on the conversion of dimethyl ether and the product selectivity were investigated under the same catalyst formulation. Results showed that a maximum conversion of dimethyl ether was obtained when a mixture consisting of 0.3 mol dimethyl ether and 120 ml acetic acid was reacted at 180 °C and 3.0 MPa for 10 h at a stirring speed of 600 rpm under a syngas flow with a CO/H 2 molar ratio of 2.5, which was catalyzed by a catalyst mixture comprising 0.3 g RhI 3 , 6g PPh 3 and1.3gCH 3 I. The selectivity of ethylidene diacetate increased with temperature, decreased with the CO/H 2 molar ratio and exhibited a maximum with pressure." @default.
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- W2020553631 date "2010-03-01" @default.
- W2020553631 modified "2023-09-27" @default.
- W2020553631 title "Synthesis of ethylidene diacetate from dimethyl ether, CO and H2" @default.
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- W2020553631 doi "https://doi.org/10.1016/s1003-9953(09)60052-9" @default.
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