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- W2020582034 abstract "X-ray and electron diffraction data have been combined to determine the unit cell for the hard domains of 4,4′-diphenylmethane diisocyanate/butanediol-based polyurethane elastomers. The analysis has been aided by manipulating digital intensity data obtained from two-dimensional densitometer scans of the diffraction patterns. A total of 22 reflections are resolved in the electron diffraction patterns, of which 11 are detected by X-rays. The unit cell is triclinic with dimensions a = 5.33, b = 5.26, c = 38.68 Å, α = 113.6, β = 116.0, γ = 94.4°. The reflections in the X-ray fibre diagrams of stretched annealed film are displaced above and below the apparent layer lines, which points to inclination of the chain axis (c) away from the direction of the draw. Refinement of coordinates of the predicted reflections shows that the c axis is tilted by 2.5° away from the direction of draw, approximately in the −1 1 1 plane." @default.
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- W2020582034 title "The hard segment unit cell for MDI-BDO-based polyurethane elastomers" @default.
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