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• W2020593586 abstract "The ruthenium N-heterocyclic carbene (NHC) hydride fluoride complexes Ru(NHC)(P–P)(CO)HF (NHC = ICy (3), IEt2Me2 (5), P–P = xantphos; NHC = ICy (7), P–P = dppf) have been prepared by treatment of the corresponding dihydride complexes [Ru(NHC)(P–P)(CO)H2] (NHC = ICy (2), IEt2Me2 (4) P–P = xantphos; NHC = ICy (6), P–P = dppf) with Et3N·3HF. In all cases, the hydride fluoride complexes exist in solution as two conformers or isomers. Although 3, 5 and 7 could be converted back to 2, 4 and 6, respectively, by heating with Et3SiH, efforts to generate a catalytic cycle for the hydrodefluorination of aromatic fluorocarbons by subsequent reaction of Ru(NHC)(P–P)(CO)H2 with C6F6 were prevented by the much more favourable cyclometallation of the carbene ligand." @default.
• W2020593586 created "2016-06-24" @default.
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• W2020593586 date "2011-02-01" @default.
• W2020593586 modified "2023-10-16" @default.
• W2020593586 title "[Ru(NHC)(P–P)(CO)HF] (NHC = N-heterocyclic carbene; P–P = xantphos, dppf) complexes: Efforts to prepare new hydrodefluorination catalysts" @default.
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• W2020593586 doi "https://doi.org/10.1016/j.jorganchem.2010.09.077" @default.
• W2020593586 hasPublicationYear "2011" @default.
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