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- W2020604804 abstract "Abstract (NBu 4 ) 2 [Pd 2 (μ-Br) 2 R 4 ] (R p -CH 3 C 6 H 4 SO 2 CH 2 ) ( 1 ) has been prepared by reaction of LiR with (NBu 4 ) 2 [Pd 2 (μ-Br) 2 Br 4 ]. Treatment of 1 with AgClO 4 in MeCN leads to the formation of [PdR 2 (NCMe) 2 ] ( 2 ). Complexes 1 and 2 are sources of complexes containing the cis -PdR 2 moiety via (a) bridge splitting reactions; (b) bridge splitting and Br − displacement; (c) MeCN displacement; or (d) metathesis with Tl(acac). A variety of anionic and neutral palladium complexes: (NBu 4 )[PdBrR 2 L] (L CN t Bu, PMePh 2 , PPh 3 or 4-Mepy); (NBu 4 ) 2 [PdR 2 (CN) 2 ]; (NBu 4 )[PdR 2 (acac)]; (NBu 4 ) 2 [Pd 2 Br 2 R 4 (μ-dppm)]; and [PdR 2 L 2 ] (L NCMe, CN t Bu, PMePh 2 , PPh 3 or 4-Mepy; L 2 = 1,5-COD, bipy, 4,4′-Me 2 bipy, dppe or dppm) has been obtained and characterized. NMR studies reveal equilibria between some of these species, and some steric hindrance to the rotation of the bulky R groups." @default.
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- W2020604804 date "1993-03-01" @default.
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- W2020604804 title "Synthesis and characterization of cis-bis[(p-tolylsulfonyl)methyl]palladium(II) complexes" @default.
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- W2020604804 doi "https://doi.org/10.1016/0022-328x(93)80284-i" @default.
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