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- W2020773334 abstract "The kinetic resolution of chlorohydrin (±)-6 has been successfully carried out via a lipase-mediated transesterification with vinyl acetate in organic as well as ionic liquid media to yield (R)-alcohol 6 and (S)-acetate 7 in high enantioselectivity. An enantioconvergent synthesis has also been achieved by a Mitsunobu esterification of a mixture of (R)-alcohol 6 and (S)-acetate 7 in one pot to convert the (R)-alcohol 6 to (S)-acetate 7. (S)-Acetate 7 has been hydrolyzed by LiOH·H2O to give epoxide (R)-2. This enantiopure epoxide has been used as a chiral precursor for the synthesis of calcilytic agent NPS-2143." @default.
- W2020773334 created "2016-06-24" @default.
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- W2020773334 creator A5085322007 @default.
- W2020773334 date "2005-08-01" @default.
- W2020773334 modified "2023-10-01" @default.
- W2020773334 title "Chemoenzymatic synthesis of calcilytic agent NPS-2143 employing a lipase-mediated resolution protocol" @default.
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- W2020773334 doi "https://doi.org/10.1016/j.tetasy.2005.07.022" @default.
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