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- W2020846039 abstract "Abstract The new complexes mer-Cr(py)3(N3)3, NaCr(py)4(N3)4, KCr(py)4(N3)4, and RbCr(py)3(N3)4 (py = pyridine) have been prepared. Infrared (4000-50 cm−1) and diffuse reflectance spectra (region 300-77 K) of powdered samples have been measured and discussed on bases of the known structures of these complexes. Single crystal absorption spectra for the mer-complex were obtained in the temperature range from 300 to 10 K revealing extensive vibronic structure associated with the 2Eg(Oh) and 2T1g(Oh) electronic origins. Crystal field calculations were used to assign the bands in the vibronic region and to obtain estimates for the crystal field and Racah parameters for this class of substances. The parameters found for the mer-complex at 10 K are 10 Dq = 17906 cm−1, B = 387 cm−1 and C = 3381 cm−1." @default.
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- W2020846039 date "1993-10-01" @default.
- W2020846039 modified "2023-09-28" @default.
- W2020846039 title "Synthesis, spectroscopic and crystal field studies on some azido-chromium(III)-pyridine complexes" @default.
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- W2020846039 doi "https://doi.org/10.1016/0584-8539(93)80121-p" @default.
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