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- W2020959067 abstract "Using the diacetate of 10-(2,5-dihydroxyphenyl)-10-hydrogen-9-oxa-10-phosphorin-10-oxide, p-acetoxy-benzoic acid, terephthalic acid and the condensation product of terephthalic acid and 1,8-octanediamine as monomers, a new kind of flame-retardant thermotropic liquid crystal copolyester containing phosphorus, nitrogen and 1,8-octanediamine softsegment (PN-TLCP) was synthesized by melt condensation polymerization. The structure and properties of PN-TLCP, such as molecular structure, texture of liquid crystal and thermal properties were investigated by fourier transform infrared spectra, X-ray diffraction, hot-stage polarizing optical microscope, differential scanning caborimetry and thermal gravimetric analysis. The results showed that the texture of PN-TLCP was the type of nematic liquid crystalline within the bounds of 180∼330°C, and its melting point was 148°C. It was proved that there were P-O and P=O stretching vibration absorption bands and C-N and C=N mixed absorption bands in Fourier transform infrared spectra of PN-TLCP. Also, the thermal stability and the char yield of PN-TLCP are favorable." @default.
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- W2020959067 date "2013-01-01" @default.
- W2020959067 modified "2023-09-28" @default.
- W2020959067 title "Synthesis and Characterization of a New Kind of Flame-Retardant Thermotropic Liquid Crystal Containing 1,8-octanediamine Softsegment" @default.
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- W2020959067 doi "https://doi.org/10.1080/03602559.2012.676136" @default.
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