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• W2021071125 abstract "[reaction in text] A novel, short, and efficient synthesis of (S)-5,5,5,5',5',5'-hexafluoroleucine (6) in greater than 99% ee starting from the protected oxazolidine aldehyde 1 is described. The enantiomeric excess of the product was calculated from an NMR analysis of a dipeptide formed by reaction with a protected L-serine derivative. Furthermore, a racemic sample of N-acylated hexafluoroleucine was enzymatically resolved by treatment with porcine kidney acylase I and was found to have the same optical rotation as a synthetic sample of 6." @default.
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• W2021071125 date "2001-04-03" @default.
• W2021071125 modified "2023-10-03" @default.
• W2021071125 title "A Novel Synthesis of Enantiomerically Pure 5,5,5,5‘,5‘,5‘-Hexafluoroleucine" @default.
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• W2021071125 doi "https://doi.org/10.1021/ol015567e" @default.
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