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- W2021127121 abstract "Abstract Dimethylamine‐tris(pentafluoroethyl)borane (C 2 F 5 ) 3 B · NHMe 2 ( 1 ) has been obtained from C 2 F 5 I, Br 2 BNMe 2 and tris(diethylamino)phosphane in sulfolane. Alkylation using CH 3 I/KOH yielded the trimethylamine‐tris(pentafluoroethyl)borane (C 2 F 5 ) 3 B · NMe 3 ( 2 ). Compound 2 reacts with NEt 3 ×3HF at 200—204 °C under replacement of the trimethylamine ligand to form the novel fluoro‐tris(pentafluoroethyl)borate anion [(C 2 F 5 ) 3 BF] — ( 3 ) in good yield. Side products are the hydroxy‐tris(pentafluoroethyl)borate [(C 2 F 5 ) 3 BOH] — ( 4 ) and the hydrido‐tris(pentafluoroethyl)borate [(C 2 F 5 ) 3 BH] — ( 5 )." @default.
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- W2021127121 date "2005-02-21" @default.
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- W2021127121 title "The New Fluoro-tris(pentafluoroethyl)borate Anion [(C2F5)3BF]?, Unexpected Formation of [(C2F5)3BH]? as a By-ProductDas neue Fluoro-tris(pentafluoroethyl)borat Anion [(C2F5)3BF]?, unerwartete Bildung des Nebenprodukts [(C2F5)3BH]?" @default.
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- W2021127121 doi "https://doi.org/10.1002/zaac.200400447" @default.
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