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- W2021304076 abstract "Abstract Sixteen methyl gem dideuterooctadecanoates with two deuterium atoms at positions 2‐ to 17‐ and seven oxo esters, 8‐oxooctadecanoate‐5,5‐ d 2 , 8‐oxooctadecanoate‐11,11‐ d 2 , 11‐oxooctadecanoate‐8,8‐ d 2 , 11‐oxooctadecanoate‐14,14‐ d 2 , 12‐oxooctadecanoate‐9,9‐ d 2 , 7‐oxooctadecanoate‐10,10‐ d 2 and 13‐oxooctadecanoate‐16,16‐ d 2 with two deuteriums on the carbon γ to the oxo group, have been synthesized. Two principal methods of introducing deuterium were used: preparation of 2,2‐dideutero acids by exchange with deuterium oxide followed by chain extension giving dideuteroxooctadecanoates, which were then reduced, as tosylhydrazones, with sodium cyanoborohydride to dideuterooctadecanoates and stepwise introduction by reduction of oxooctadecanoates with sodium borodeuteride, formation of tosylate or mesylate, reduction with lithium aluminium deuteride to tetradeuterooctadecanol and oxidation to dideuterooctadecanoic acid." @default.
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- W2021304076 date "1977-01-01" @default.
- W2021304076 modified "2023-09-30" @default.
- W2021304076 title "Preparation of specifically dideuterated octadecanoates and oxooctadecanoates" @default.
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- W2021304076 doi "https://doi.org/10.1007/bf02532978" @default.
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