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• W2021320557 abstract "This manuscript demonstrates the synthesis of glassy polymer network isomers to control morphological variations and study solvent ingress behavior independent of chemical affinity. Well-controlled network architectures with varying free volume average hole-sizes have been shown to substantially influence solvent ingress within glassy polymer networks. Bisphenol-A diglycidyl ether (DGEBA), bisphenol-F diglycidyl ether (DGEBF) and tetraglydicyl-4,4′-diamino-diphenyl methane (TGDDM) were cured with 3,3′- and 4,4′-diaminodiphenyl sulfone (DDS) at a stoichiometric ratio of 1:1 oxirane to amine active hydrogen to generate a series of network architectures with an average free volume hole-size (Vh) ranging between 59 and 82 Å3. Polymer networks were exposed to water and a broad range of organic solvents ranging in van der Waals (vdW) volumes from 18 to 88 Å3 for up to 10,000 h time. A clear relationship between glassy polymer network Vh and fluid penetration has been established. As penetrant vdW volume approached Vh uptake kinetics significantly decreased, and as penetrant vdW volume exceeded Vh a blocking mechanism dominated ingress and prevented penetrant transport. These results suggest that reducing the free volume hole-size is a reasonable approach to control solvent properties for glassy polymer networks." @default.
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• W2021320557 date "2011-09-01" @default.
• W2021320557 modified "2023-09-30" @default.
• W2021320557 title "Effect of free volume hole-size on fluid ingress of glassy epoxy networks" @default.
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• W2021320557 doi "https://doi.org/10.1016/j.polymer.2011.07.042" @default.
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