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- W2021361853 abstract "A general, mild and efficient protocol for the synthesis of ethyl 4-methyl-2-(thiophen)-2,5-dihydro-1,5-benzodiazepine-3-carboxylate is achieved for first time using H3PMo12O40 in ethanol at 0 °C by a one-pot, three-component condensation of various thiophene aldehydes, substituted o-phenylenediamines and ethyl acetoacetate. Compared with the conventional synthesis method, this procedure has the advantages of convenient operation, excellent yields, and environmentally benign. A plausible formation mechanism has been proposed. The structure of the products is characterized by 1H NMR, IR, MS and elemental analysis." @default.
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- W2021361853 date "2014-02-01" @default.
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- W2021361853 title "Highly efficient one-pot, three-component synthesis of 1,5-benzodiazepine derivatives" @default.
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- W2021361853 doi "https://doi.org/10.1016/j.cclet.2013.11.035" @default.
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