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- W2021697576 abstract "Well-crystal macrocyclic (arylene thioether ketone) oligomers were synthesized under high dilution condition by the reaction of Na2S with bis(4-fluoro-phenyl)-methanone in 1-methyl-pyrrolidone (NMP). The oligomers were fully characterized by Matrix-assisted laser desorption/ionization time-of-flight mass spectra (MALDI-TOF-MS), high-pressure liquid chromatography (HPLC), gel permeation chromatography (GPC), 1H NMR, 13C-NMR, and differential scanning calorimetry (DSC). According to DSC studies, uncatalyzed and rapid ring-opening polymerization (ROP) of the oligomers took place instantly when they were heated to melting point. Extracted by dichloro-methane, the obtained polymer neither loses any weight nor dissolves in boiling 1-chloro- naphthalene. These facts indicated that there are no residual oligomers within the resultant polymer. The as-prepared oligomers could be potentially used as high-temperature hot-melt adhesive at a high temperature > 350°C, and matrices for high-performance composites and nanocomposites. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 100: 161–166, 2006" @default.
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- W2021697576 date "2006-01-01" @default.
- W2021697576 modified "2023-09-23" @default.
- W2021697576 title "One step synthesis and rapid ring-opening polymerization of macrocyclic (arylene thioether ketone) oligomers" @default.
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- W2021697576 doi "https://doi.org/10.1002/app.22642" @default.
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