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- W2021804601 abstract "Abstract Equimolar quantities of [WI2 (CO)3(NCMe)2] and pyridine-2-thione (pySH) or pyrimidine-2-thione (pymSH) react in CH2CI2 at room temperature to give the dimeric complexes [{W(μ-I)I(CO)3 (pySH)}2] (1) or [{W(μ-I)I(CO)3(pymSH)}2]· 1/2CH2CL2 (2), respectively. Reaction of [MI2(CO)3(NCMe)2] (M = Mo or W) with two equivalents of pySH (for M = Mo only) or pymSH in CH2Cl2 afforded the bis(ligand) complexes [MoI2(CO)3(pySH)2] (3), [MoI2(CO)3(pymSH)2] (4) or [WI2(CO)3(pymSH)2] · CH2Cl2 (5) respectively. Reaction of [WI2(CO)3(NCMe)2] with two equivalents of PPh3 or one equivalent of Ph2P(CH2)nPPh2 (n = 1 to 6) in CH2Cl2 at room temperature, followed by an in situ reaction with one equivalent of pySH yielded the cationic complexes [WI(CO)3(PPh3)2(pySH)]I (6) or [WI(CO)3{Ph2P(CH2)nPPh2}(pySH)]I (7→12), respectively." @default.
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- W2021804601 date "1995-05-01" @default.
- W2021804601 modified "2023-09-25" @default.
- W2021804601 title "SEVEN-COORDINATE PYRIDINE-2-THIONE AND PYRIMIDINE-2-THIONE COMPLEXES OF MOLYBDENUM (II) TUNGSTEN (II)" @default.
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