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• W2022067802 abstract "The structure of the metastable form I polymorph of the macrolide antibiotic clarithromycin, C 38 H 69 NO 13 , was determined by a powder diffraction method using synchrotron radiation. The space group of form I is P 2 1 2 1 2. The initial model was determined by a molecular replacement method using the structure of clarithromycin form 0 as a search model, and the final structure was obtained through Rietveld refinements. In the form I crystal structure, the clarithromycin molecules are aligned parallel along the a axis in a head-to-tail manner with intermolecular hydrogen bonds between the hydroxy O atoms. The dimethylamine groups of the clarithromycin molecule interdigitate between neighbouring head-to-tail clarithromycin alignments. The novel crystal packing found in form I provides a mechanism that describes the transformation of form 0 to form I." @default.
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• W2022067802 date "2012-01-06" @default.
• W2022067802 modified "2023-10-16" @default.
• W2022067802 title "Clarithromycin form I determined by synchrotron X-ray powder diffraction" @default.
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• W2022067802 doi "https://doi.org/10.1107/s0108270111054230" @default.
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