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- W2022070157 abstract "Lithium–calcium alanate, LiCa(AlH4)3, was synthesized by a mechano-chemically activated reaction of LiAlH4 with CaCl2 in a molar ratio of 3:1. The results of X-ray diffraction (XRD) and Fourier transform infra-red (FTIR) spectroscopy indicated that the reactants converted entirely into LiCa(AlH4)3 accompanied with a by-product LiCl after 30 h ball-milling. LiCa(AlH4)3 crystallized in a hexagonal structure with space group P63/m (No. 176), and with cell parameters a = b = 8.9197(12) and c = 5.8887(7) Å. Thermal decomposition of LiCa(AlH4)3 initiated around 120 °C and proceeded mainly in three steps. The first two steps could be assigned to the formation of CaH2, LiH and Al, with LiCaAlH6 as a possible intermediate, and the third step was the further formation of some CaAl intermetallic phases." @default.
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- W2022070157 date "2012-04-01" @default.
- W2022070157 modified "2023-09-24" @default.
- W2022070157 title "Synthesis, crystal structure and thermal decomposition of LiCa(AlH4)3" @default.
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- W2022070157 doi "https://doi.org/10.1016/j.jallcom.2012.01.011" @default.
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