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• W2022088182 abstract "Nanofabrication of crystalline materials has been well recognised as one of the most efficient pathways to improve the electrochemical performance of an electrode on the principle of lithium-ion insertion/extraction depth. Herein, it is reported that freshly prepared β-MnO2 nanorods have been successfully used as sacrificial templates to synthesise the rod-like spinels of pristine LiMn2O4 with high purity and good crystallinity. Under the optimum sintering temperature of 750°C for 10 h, the presence of doping reactant Ni(CH3COO)2·4H2O can greatly weaken the templating effectiveness of β-MnO2 nanorods, effectively resulting in LiNixMn2−xO4 (x=0.025, 0.05 and 0.1) samples with a relatively short aspect ratio. Galvanostatic charge–discharge tests showed that the undoped rods could acquire an initial discharge capacity of 125.9 mAh/g at 1 C and the corresponding capacity retention of 75.3% after 100 cycles. Interestingly, with the increase of element-doped amount, the resulting LiNixMn2−xO4 displayed a gradually improved cyclability at the charge–discharge rate of 1 C at room temperature." @default.
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• W2022088182 date "2012-01-01" @default.
• W2022088182 modified "2023-09-22" @default.
• W2022088182 title "Sacrificial templating synthesis of rod-like LiNixMn2−xO4 spinels and their improved cycling performance" @default.
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• W2022088182 doi "https://doi.org/10.1049/mnl.2012.0020" @default.
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