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• W2022123925 abstract "Abstract Electrochemical lithium insertion in pure and (PTFE-and/or C-) mixed CdIn 2 S 2 Se 2 has been investigated by galvanostatic discharge experiments in the (−) Li/organic electrolyte/CdIn 2 S 2 Se 2 (+) cell, also considering the behaviour in quasi-equilibrium open-circuit conditions, and by cyclic voltammetry. Structural changes induced by lithium insertion have been observed by powder X-ray diffraction measurements. The reversibility of the process is poor in the whole range explored, but differences in behaviour are noticed. During a galvanostatic discharge of the cell up to about 0.7 F.mol −1 no structural change takes place and the lithium diffusion process is slow, as shown by the very low value of the chemical diffusion coefficient (around 10 −12 cm 2 .s −1 , at 30 °C) determined according to a current-pulse relaxation technique. During a deeper discharge up to 5.35 F.mol −1 two plateaux — a short and an extended one — are noted in the experimental curve, while pseudocrystalline phases are formed. As a consequence of these structural rearrangements, the time needed to reach open-circuit quasi-equilibrium conditions after a galvanostatic discharge is high, particularly in the region of the first plateau. Analyses of the results evidence that CdIn 2 S 2 Se 2 is a very interesting new compound, more significant for its fundamental properties than in view of its application as cathode material in aprotic solvent lithium cells." @default.
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• W2022123925 date "1988-05-01" @default.
• W2022123925 modified "2023-09-23" @default.
• W2022123925 title "Electrochemical and structural aspects of lithium insertion into the new layered compound CdIn2S2Se2" @default.
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• W2022123925 doi "https://doi.org/10.1016/0254-0584(88)90098-3" @default.
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