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• W2022142719 endingPage "187" @default.
• W2022142719 startingPage "180" @default.
• W2022142719 abstract "The azodye ligand (HL(1)) was synthesized from the coupling of sulfaguanidine diazonium salt with 2,4-dihydroxy-benzaldehyde while the two ligands, HL(2) and HL(3), were prepared by the coupling of sulfadiazine diazonium salt with salicylaldehyde (HL(2)) and 2,4-dihydroxy-benzaldehyde (HL(3)). The prepared ligands were characterized by elemental analysis, IR, (1)H NMR and mass spectra. Cu(II), Co(II) and Ni(II) complexes of the prepared ligands have been synthesized and characterized by various spectroscopic techniques like IR, UV-Visible as well as magnetic and thermal (TG and DTA) measurements. It was found that all the ligands behave as a monobasic bidentate which coordinated to the metal center through the azo nitrogen and α-hydroxy oxygen atoms in the case of HL(1) and HL(3). HL(2) coordinated to the metal center through sulfonamide oxygen and pyrimidine nitrogen. The applications of the prepared complexes in the oxidative degradation of indigo carmine dye exhibited good catalytic activity in the presence of H2O2 as an oxidant. The reactions followed first-order kinetics and the rate constants were determined. The degradation reaction involved the catalytic action of the azo-dye complexes toward H2O2 decomposition, which can lead to the generation of HO radicals as a highly efficient oxidant attacking the target dye. The detailed kinetic studies and the mechanism of these catalytic reactions are under consideration in our group." @default.
• W2022142719 created "2016-06-24" @default.
• W2022142719 creator A5005647867 @default.
• W2022142719 creator A5066627191 @default.
• W2022142719 creator A5069714565 @default.
• W2022142719 creator A5071481591 @default.
• W2022142719 date "2014-03-01" @default.
• W2022142719 modified "2023-09-26" @default.
• W2022142719 title "Synthesis and characterization of Cu(II), Co(II) and Ni(II) complexes of a number of sulfadrug azodyes and their application for wastewater treatment" @default.
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• W2022142719 doi "https://doi.org/10.1016/j.saa.2013.09.070" @default.
• W2022142719 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/24239761" @default.
• W2022142719 hasPublicationYear "2014" @default.
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