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• W2022148517 startingPage "11665" @default.
• W2022148517 abstract "The influence of the chemical composition and of the storage and activation protocol on the diffusion of methanol into strongly chemically zoned crystals of the silicoaluminophosphate zeotype STA-7 has been investigated by interference microscopy. Analysis of the evolution of transient intracrystalline concentration profiles reveals that just-calcined SAPO STA-7 crystals with lower Si content (Si/(Si + P) = 0.18) exhibit higher surface permeability and bulk diffusivity than those with higher Si content (S/(Si + P) = 0.37). Remarkably, crystals with the higher Si content which were stored in the calcined form crack during activation along planes of weakness already present in the as-prepared crystals, creating fresh surfaces through regions of lower Si that are much more easily penetrated by the adsorbing methanol than are the original surfaces." @default.
• W2022148517 created "2016-06-24" @default.
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• W2022148517 date "2010-08-03" @default.
• W2022148517 modified "2023-09-24" @default.
• W2022148517 title "Assessing Molecular Transport Properties of Nanoporous Materials by Interference Microscopy: Remarkable Effects of Composition and Microstructure on Diffusion in the Silicoaluminophosphate Zeotype STA-7" @default.
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• W2022148517 doi "https://doi.org/10.1021/ja104016n" @default.
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