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- W2022153732 abstract "Für NMR-spektrometrische Konformationsanalysen wurden fünf unterschiedlich deuterierte Pentapeptidlactone (9a–e) und daraus vier selektiv nur im (α)- bzw. (β)-Peptidteil deuterierte Actinomycin C1-säure-lacton-Paare (12, 13) sowie einige in beiden Peptid-Gruppen jeweils gleich markierte iso-Deutero-actinomycine (15) aufgebaut. Lactonisierung von 12, 13 gab acht stellungsspezifisch in (α) oder (β) markierte aniso-Deutero-actinomycine C1 (16, 17). Über 15–17 gelang erstmals die (α, β)-stellungsspezifische Zuordnung der NMR-Signale von Actinomycin C1(D) (2) und eng damit verwandten Actinomycinen wie z. B. C2, i-C2 und C3. Syntheses of Selectively Deuterated Pentapeptide Lactones and Actinomycines Specifically Labelled in the (α)- or (β)-Peptide Ring For n.m.r. spectroscopic conformational analysis five diversely deuterated pentapeptide lactones (9a–e) and derived from them four pairs of actinomycine C1-acid lactones (12, 13) selectively deuterated only in the (α)- or (β)-peptide chain, as well as some iso-deuteroactinomycines (15) equally labelled in both peptides were synthesized. Lactonization of 12, 13 yielded eight aniso-deutero-actinomycines C1 (16, 17) specifically deuterated in (α) or (β). By use of 15–17 structure specific assignments of the n.m.r. signals from actinomycine C1(D) (2) and closely related actinomycines (C2, i-C2, C3 etc.) could be achieved." @default.
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- W2022153732 date "1971-11-01" @default.
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- W2022153732 title "Synthesen von selektiv deuterierten Pentapeptidlactonen und stellungsspezifisch in (α)‐ oder (β)‐Peptidring markierten Actinomycinen" @default.
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- W2022153732 doi "https://doi.org/10.1002/cber.19711041131" @default.
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