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• W2022164806 abstract "A new synthesis is described for the production of the positron emitting radiopharmaceutical R-(+)-7-chloro-8-hydroxy-2,3,4,5-tetrahydro-3-N-[11C]methyl-1-phenyl-1H-3-benzazepine (SCH 23390, 2a). This novel method involves reductive carboxylation, in which [11C]CO2 is reacted with the trimethylsilyl derivative of the desmethyl compound (SCH 24518, 1a) followed by treatment with lithium aluminum hydride, to afford no carrier added11C-labeled SCH 23390. The procedure gave chemically and radiochemically pure 11C-labeled SCH 23390 in 53–72% radiochemical yield with an unoptimized specific activity of 40 Ci/mmol within 45–50 min from the end of bombardment." @default.
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• W2022164806 date "1989-01-01" @default.
• W2022164806 modified "2023-10-09" @default.
• W2022164806 title "Synthesis of the labeled D1 receptor antagonist SCH 23390 using [11C]carbon dioxide" @default.
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• W2022164806 doi "https://doi.org/10.1016/0883-2889(89)90210-4" @default.
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