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• W2022179117 abstract "A fundamentally new single-walled and multiwalled carbon nanotube sidewall functionalization technique has been developed in which solvent is not required and the reaction times are greatly shortened (1 h at 60 degrees C). Exploiting the long linear dimension of the nanotube ropes by macroscopic mechanical deformation, reactive sites are generated merely by mechanically deforming the tubes using a stir bar. This approach eliminates the need for large volumes of solvent ( approximately 2 L/g), which were formerly considered essential due to the insolubility of carbon nanotubes. Using a series of 4-substituted anilines and a nitrite, the aryl diazonium intermediates were generated in situ and permitted to react with the tubes. Raman, IR, and UV spectroscopies, coupled with thermogravimetric analyses and solubility studies, support the assignments." @default.
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• W2022179117 date "2003-01-09" @default.
• W2022179117 modified "2023-10-16" @default.
• W2022179117 title "Solvent-Free Functionalization of Carbon Nanotubes" @default.
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• W2022179117 doi "https://doi.org/10.1021/ja0289806" @default.
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