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• W2022236264 abstract "A new supramolecular compound [Zn(H 2 EDTA)(H 2 O)](Q) 2 (H 2 O) 2 ( 1 ), where H 4 EDTA=ethylenediaminetetraacetic acid and Q=4-(carboxylate)pyridinium, has been prepared by mild hydrothermal reaction and characterized by elemental analysis, IR spectrum and thermogravimetric analysis. Single-crystal X-ray diffraction of 1 [monoclinic, space group C2 / c , a =11.310(4) Å, b =9.704(4) Å, c =23.798(10) Å, β =97.401(10)°, Z =4] revealed that the Zn II ion coordinates to the chelating tetradentate ligand H 2 EDTA and a water molecule, taking a distorted trigonal-bipyramid geometry. The mononuclear [Zn(H 2 EDTA)(H 2 O)] subunits are linked to form two-dimensional layered architectures by the lattice water moieties through O–H⋯O hydrogen bonds, which are further extended to a three-dimensional (3D) supramolecular network by 4-(carboxylate)pyridinium guests (resulting from the ring-opening hydrolysis of 2,5-bis(4-pyridyl)-1,3,4-oxadiazole) through extensive hydrogen-bonding interactions. The 3D supramolecular framework is also stabilized by significant face-to-face π–π stacking interactions between the aromatic pyridinium systems." @default.
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• W2022236264 date "2004-09-01" @default.
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• W2022236264 title "Hydrothermal synthesis, characterization and crystal structure of a three-dimensional (3D) ZnII supramolecular compound with ethylenediaminetetraacetic acid ligand and 4-(carboxylate)pyridinium guests" @default.
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• W2022236264 doi "https://doi.org/10.1016/j.molstruc.2004.05.027" @default.
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