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- W2022245843 abstract "The synthesis of 1,1,3,3-tetraethoxypropane-1,2,3-14C3 from uniformly labeled paraldehyde is described. The synthesis involves three steps and proceeds in an overall yield of 25%. The final product is greater than 95% radiochemically pure and it is stable indefinitely when stored as thoroughly degassed benzene solutions. Hydrolysis of radiolabeled tetraethoxypropane occurs in moderate yields to form malondialdehyde-1,2,3-14C3(1,3 propanedial-1,2,3-14C3) which is isolated and stored as the sodium salt. One of the intermediates in the synthesis of tetraethoxypropane is ethyl vinyl-[1,2-14C2] ether, which is isolable in 50% overall yield from paraldehyde. The widespread utilization of ethyl vinyl ether in organic synthesis suggests that the radiolabeled material should provide an entry to a large number of specifically [14C] labeled compounds." @default.
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- W2022245843 date "1980-09-01" @default.
- W2022245843 modified "2023-09-25" @default.
- W2022245843 title "Synthesis of malondialdehyde-1,2,3-14C3 via ethyl vinyl-[1,2-14C2] ether" @default.
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- W2022245843 doi "https://doi.org/10.1002/jlcr.2580170502" @default.
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