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- W2022272458 abstract "The controlled synthesis of Pd icosahedra in tetraethylene glycol with H2PdCl4 as a precursor and polyvinylpyrrolidone (PVP) as a stabilizer was demonstrated. Tetraethylene glycol served as both solvent and reducing agent, and uniform Pd icosahedra with a mean size of 45 ± 5 nm were successfully synthesized with a high yield of over 90% in oil-bath at 160 °C for 2.5 h. A certain affinity for the metal particles, a higher viscosity and a milder reducing power of tetraethylene glycol would be responsible for the formation of uniform and stable Pd icosahedra with a high yield. The optimum KOH/Pd(II) ratio, PVP/Pd(II) ratio, temperature, and heating time for the reaction system was 1.4/1, 1/1, 160 °C, and 2.5 h, respectively." @default.
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- W2022272458 date "2009-09-01" @default.
- W2022272458 modified "2023-09-26" @default.
- W2022272458 title "Controlled synthesis of palladium icosahedra nanocrystals by reducing H2PdCl4 with tetraethylene glycol" @default.
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- W2022272458 doi "https://doi.org/10.1016/j.colsurfa.2009.07.007" @default.
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