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- W2022272551 abstract "The reduction of CrCl3 by zinc dust in THF solution followed by slow addition to an ethanolic solution K(acacen) gave a brown powder, which when reacted with pyridine produced an intractable brown tar. Careful recrystallization of the tat from methanol gave a small quantity of crystalline [Cr(acacen)py2][ZnCl3py]. The structure consists of a set of two crystallographically independent complex cations and anions of the above formula. Crystal data: monoclinic space group P21, a=12.667(4), b=16.146(4), c=16.262(5) Å, β=108.57(1)°, V=3153(2) Å3, Z=4. A total of 7657 reflections was collected with graphite monochromated Mo Kα radiation (to 20=54°), of which 4536 were used in subsequent structure solution and refinement (I ⩾ 3σ(I)). The structure was solved by direct methods, and least-squares refinement converged at R=0.037." @default.
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- W2022272551 date "1994-03-01" @default.
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- W2022272551 title "The synthesis and crystal structure of [Cr(acacen)py2] [ZnCl3py]" @default.
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- W2022272551 doi "https://doi.org/10.1016/0020-1693(93)03745-v" @default.
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