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- W2022279868 abstract "A stereocontrolled synthesis of ()-isocomene (1) via selective monoketalization of tricyclo[6.3.0.]undeca-4,7-dione(13) was reported. Grignard reaction of bicyclic enone 10, which was prepared from 2-methyl-1,3-cyclopentadione, gave the 1,4-addition product 11. The subsequent aldol condensation product 12 was converted to mesyl derivative 13. Transformation from 13 to the desired product 19 was achieved by a series of reactions, i.e., the selective monoketalization at C-4 carbonyl group, the elimination of a mesyl group, Birch alkylation, methylation at C-6, the reduction of carbonyl group, the dehydration of alcohol 18, and hydrolysis of the ketal group." @default.
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- W2022279868 date "2010-08-22" @default.
- W2022279868 modified "2023-09-26" @default.
- W2022279868 title "ChemInform Abstract: Formal Synthesis of Isocomene." @default.
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- W2022279868 doi "https://doi.org/10.1002/chin.199208279" @default.
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