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- W2022286165 abstract "Abstract Electron impact spectra of isomeric 7-oxabicyclo[4.3.0]nonanes differ in the relative abundance of (M-H)+ ions. The critical energy of the angular hydrogen loss from the trans-annulated isomer 1 is lower by 9–10 kcal mol−1 than that of the cis-isomer 2, due to stereoelectronic assistance of the neighbouring oxygen pz orbital in the cleavage of the C(6)-H bond in 1XXX. High kinetic energy released during the hydrogen loss from 2XXX, [T] = 7.5 kcal mol−1, is consistent with non-relaxed geometry of the resulting (M-H)+ ion. Isomeric 2-oxabicyclo[4.4.0]decanes show analogous although smaller differences than 1 and 2. Photoelectron, electron impact, metastable and collision induced decomposition mass spectra are reported." @default.
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- W2022286165 title "Stereoelectronic control of ion fragmentations: loss of hydrogen from cyclic ethers during electron impact mass spectrometry" @default.
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