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- W2022307926 abstract "High aspect ratio nickel microfluidic columns were fabricated using the LiGA technique. The 2-m-long 50-mum-wide high aspect ratio columns will be the separation component of a handheld gas chromatograph device for detecting semivolatile and volatile compounds. As a first step, 600-mum-deep electrodeposited nickel columns were fabricated. The serpentine columns were sealed and pressure-flow rate characteristics compared with the theoretical values. The response of the sealed columns was studied by running methane gas plugs through uncoated columns with a flame ionization detector at the exit. Negligible flow-induced dispersion was observed in the sealed metal columns. Unretained peak widths of ~15 ms were measured, and the experimental pressure and flow rate distributions matched those predicted by established analytical models within plusmn2.5%. Columns were coated with OV-1 stationary phase using static coating methods. A mixture of four hydrocarbons C6, C8, C10, and C12 was separated in a coated 50 mum by 600 mum by 0.5 m column in less than 2 s at 70 degC" @default.
- W2022307926 created "2016-06-24" @default.
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- W2022307926 date "2007-04-01" @default.
- W2022307926 modified "2023-09-27" @default.
- W2022307926 title "Fabrication and Preliminary Results for LiGA Fabricated Nickel Micro Gas Chromatograph Columns" @default.
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- W2022307926 doi "https://doi.org/10.1109/jmems.2007.892903" @default.
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