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- W2022331111 abstract "Abstract The oxidative addition of aryl-halogen bonds of Schiff bases (2-ClC6H4CHNCH2)2 (1), (2-BrC 6H4CHNCH2)2 (2), 1,4-(2-BrC6H4CHN)2C6H4 (3), 4,4′-(2-BrC6H4CHNC6H4)2 (4 and the azine (2-BrC6H4CHN)2 (5 to Pd(dba)2 has been carried out in benzene. Insoluble halogeno-bridged polymeric complexes [{ Pd(C 6 H 4 CHN CH 2 )Cl} n ] (1a), [{ Pd(C 6 H 4 CHN CH 2 )Br} n ] (2a), [1,4-{Br Pd(C 6 H 4 CHN C 6 H 4 NCHC 6 H 4 )Pd Br} n ] (3a), [4,4′-{ Pd(C 6 H 4 CHN C 6 H 4 )Br} n ] (4a) and [{ Pd(C 6 H 4 CHN C 6 H 4 )Br} n ] (5a) were formed. The bridge-splitting reactions of halogeno-bridged complexes were studied with different ligands like triphenylphosphine, triethylphosphite, 4-picoline, diethyldithiocarbamate and N-(2-hydroxy)benzylideneamine. All the double cyclopalladated complexes obtained were analysed by means of 1H NMR and 13C NMR spectroscopy." @default.
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- W2022331111 date "1995-08-01" @default.
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- W2022331111 title "Synthesis and characterization of double cyclopalladated complexes of Schiff bases and azine—oxidative addition of aryl-halogen bond" @default.
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