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- W2022333610 abstract "Abstract The reaction of [Nb(NMe2)3(N-2,6-iPr2C6H3)] 1 with the cyclopentadienyl-indenyl isopropylidene ligand 2 gave the new half-sandwich niobium complex [Nb(η5- C5H4R)(NMe2)2(N-2,6-iPr2C6H3)] (R=CMe2C9H7) 3 in high yield. The new ansa-type niobiocene [Nb(NMe2)(N-2,6-i-Pr2C6H3)(η5:η1-{C5H4}C(CH3)2{C9H6}] 4 was obtained at higher temperatures by an intramolecular deprotonation with concomitant coordination of the indenyl group. The reactivity of the new ansa-niobiocene 4 towards electrophilic reagents, giving chloro- and cationic ansa-type niobium complexes is described." @default.
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- W2022333610 date "1998-07-01" @default.
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- W2022333610 title "Half-sandwich and ansa-niobiocenes: synthesis and reactivity" @default.
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