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- W2022336483 abstract "Abstract The infrared spectra of normal and deuterated ice prepared by freezing the liquid or by condensing the vapor were studied at temperatures down to −190°C. No important spectral differences between the various specimens were found. The infrared spectra of H2O, HDO and D2O at −190°C were compared and the spectrum of crystalline HOD identified. Starting from the HOD spectrum the spectra of H2O and D2O could be clarified. The band at 2230 cm−1 in ice is identified as the second overtone of a librational mode. The stretching region of ice consists of 2ν2 at about 3150 cm−1, ν3 at about 3240 cm−1 and ν1 at about 3350 cm−1; D2O is analogous. The cross-over between the frequency of ν1 and ν3 in passing from gas to solid is caused by a change in the stretch-stretch interaction constant. Its magnitude in ice,f12 = 0.3 cm dyn A , can be roughly explained on electrostatic grounds. The spectrum of the overtone region shows that the barrier to proton transfer in ice is greater than 27 kcal mole ." @default.
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- W2022336483 date "1958-10-01" @default.
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- W2022336483 title "The infrared spectra of crystalline H2O, D2O and HDO" @default.
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- W2022336483 doi "https://doi.org/10.1016/0371-1951(58)80060-0" @default.
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