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- W2022346067 abstract "Abstract A method is described for using isotope dilution to determine both the amount of natural zinc and enriched isotopes of zinc in biological samples. Isotope dilution inductively coupled plasma mass spectrometry offers a way to quantify not only the natural zinc found in a sample but also the enriched isotope tracers of zinc. Accurate values for the enriched isotopes and natural zinc are obtained by adjusting the mass count rate data for measurable instrumental biases. Analytical interferences from the matrix are avoided by extracting the zinc from the sample matrix using diethylammonium diethyldithiocarbamate. The extraction technique separates the zinc from elements which form interfering molecular ions at the same nominal masses as the zinc isotopes. Accuracy of the method is verified using standard reference materials. The detection limit is 0.06 μg Zn per sample. Precision of the abundance ratios range from 0.3–0.8% R.S.D. for natural zinc concentrations of about 200–600 μ g−1. The accuracy and precision of the measurements make it possible to follow enriched isotopic tracers of zinc in biological samples in metabolic tracer studies." @default.
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- W2022346067 date "1992-03-01" @default.
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- W2022346067 title "Determination of zinc stable isotopes in biological materials using isotope dilution inductively coupled plasma mass spectrometry" @default.
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- W2022346067 doi "https://doi.org/10.1016/0003-2670(92)85107-h" @default.
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