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- W2022350039 abstract "X-ray diffractometry (XRD) and X-ray photoelectron spectroscopy (XPS) were used to characterise titanium nitride phases in a Ti–6Al–4V alloy at different depths, produced by laser nitriding with spinning and stationary beams. The XPS results showed, via deconvolution methods, that the line shapes and peak positions of Ti2p are dependent upon the nitrogen concentration at different depths and were able to provide more precise information on the TiNx substoichiometry. XRD and XPS have led to the conclusion that with a spinning beam, the large dendritic structure which formed in Zone 1, about 50 μm depth, consisted of TiN0.80 on the top surface and TiN0.85 at a depth of 35 μm; a needle-like structure which formed in Zone 2, about 350 μm below the surface, consisted of TiN0.3 and martensitic α′-Ti. With a stationary beam, the large dendritic structure was TiN0.75 on the top surface and TiN0.50 (cubic) in the melt pool below 50 μm depth; also in the melt pool were TiN0.3 and martensitic α′-Ti phases." @default.
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- W2022350039 date "1998-03-01" @default.
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- W2022350039 title "Surface analytical studies of a laser nitrided Ti–6Al–4V alloy: a comparison of spinning and stationary laser beam modes" @default.
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- W2022350039 doi "https://doi.org/10.1016/s1359-6454(97)00438-2" @default.
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