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- W2022354914 abstract "Abstract The kinetics of crystallization of Pb 15 Ge 27 Se 58 was studied by differential scanning calorimetry non-isothermally. Various experimental methods are currently employed for determining the kinetic parameters of crystallization in a glassy system. These parameters include the activation energy of crystallization E (kJ/mol), the kinetic exponent n and the frequency factor K o (s −1 ). Recently, a new method (VHR method) has been derived from Johnson–Mehl–Avrami (JMA) transformation rate equation to calculate – in sequence – the crystallization kinetic parameters of a glassy system. The VHR technique has been used to estimate the crystallization parameters of Pb 15 Ge 27 Se 58 chalcogenide glass under non-isothermal conditions. The average value of E , n and K o are found equal to 181.74 ± 0.58 (kJ/mol), 1.085 ± 0.023 and (9.196 ± 0.716) × 10 12 (s −1 ), respectively. The kinetic exponent, n ≈ 1 indicates a surface nucleation mechanism." @default.
- W2022354914 created "2016-06-24" @default.
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- W2022354914 date "2010-01-01" @default.
- W2022354914 modified "2023-09-30" @default.
- W2022354914 title "Crystallization kinetics determination of Pb15Ge27Se58 chalcogenide glass by using the various heating rates (VHR) method" @default.
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- W2022354914 doi "https://doi.org/10.1016/j.jnoncrysol.2009.10.010" @default.
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