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- W2022379757 abstract "The synthesis of 5,5,10,10-tetramethyl-1-oxacyclotridecan-6,7,8,9-tetrone (12) was achieved via a multistep procedure involving an oxidation known as the Rubottom reaction. The key intermediates were the dialdehyde (25), the diacid (33), the cyclic diketone (39) and the bis(silyl enol ether) (42). The oxidation of 42 with mCPBA yielded two diastereomers, the syn and anti bis(α-hydroxy ketones) (44, 45) the ratio of which depends strongly on the solvent used. This result combined with the isolation of the diepoxide (43) gives an insight into the stereochemistry of the Rubottom reaction." @default.
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- W2022379757 date "1995-09-01" @default.
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- W2022379757 title "Synthesis of 5,5,10,10-tetramethyl-1-oxacyclotridecane-6,7,8,9-tetrone – on the mechanism of the Rubottom reaction" @default.
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- W2022379757 doi "https://doi.org/10.1002/jlac.1995199509230" @default.
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