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- W2022381162 abstract "Self-assembled superstructures resulting from the competition between crystallization and microphase separation of semicrystalline poly(styrene)-b-poly(l-lactide) (PS−PLLA) chiral block copolymers (BCPs*) were examined. A kinetically controlled process by changing nonsolvent addition rate was utilized to control the BCP* self-assembly. Single-crystal lozenge lamellae were obtained by the slow self-assembly (i.e., slow nonsolvent addition rate) of PS−PLLA BCP* with long PS chain (i.e., PS-rich PS−PLLA BCP*) whereas amorphous helical ribbon superstructures were obtained from the fast self-assembly (i.e., fast nonsolvent addition rate). Moreover, amorphous flat ribbon superstructures were obtained in achiral BCPs, poly(styrene)-b-poly(dl-lactide) (PS−PLA), suggesting that the chirality plays an important role in the formation of the helical ribbon superstructures. By contrast, the self-assembly of PS−PLLA BCP* with short PS chain (i.e., PLLA-rich PS−PLLA BCP*) was dominated by PLLA crystallization regardless of the variation of nonsolvent addition rate, indicating that the PLLA crystallization rate is dependent upon the length of PS chain in PS−PLLA BCPs*. As a result, the formation of helical architectures from the self-assembly of PS−PLLA BCP* reflects the impact of chirality on microphase separation, but the chiral effect might be overwhelmed by crystallization." @default.
- W2022381162 created "2016-06-24" @default.
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- W2022381162 date "2010-08-16" @default.
- W2022381162 modified "2023-09-25" @default.
- W2022381162 title "Kinetically Controlled Self-Assembled Superstructures from Semicrystalline Chiral Block Copolymers" @default.
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- W2022381162 doi "https://doi.org/10.1021/ma1009879" @default.
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