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- W2022385542 abstract "Abstract Complexation of a “hybrid” tripodal ligand 2,2-bis(diphenylphosphinomethyl)-1-methoxypropane ( P 2 O ) with group VI carbonyls, nickel(II) and palladium(II) compounds has been studied. Thus P 2 O reacts with M(CO) 6 , NiCl 2 and PdCl 2 to give ( P 2 O )M(CO) 4 (M = Cr, Mo, W), ( P 2 O )NiCl 2 and ( P 2 O )PdCl 2 , respectively. All the complexes have been characterized by spectroscopy and elemental analysis, and the crystal structures of the complexes of ( P 2 O )Mo(CO) 4 ( 4b ), ( P 2 O )W(CO) 4 ( 4c ) and ( P 2 O )NiCl 2 ( 6 ) have been determined by X-ray diffraction. In all cases, the tripodal ligand behaves solely as a bidentate with two phosphorus donors coordinating to the metal centers. In the examination of the conformations of the six-membered chelate rings, it was found that both 4b and 4c were in the twisted-boat form; whereas 6 was in the chair form. The possible reasons for this conformational difference are discussed." @default.
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- W2022385542 date "1990-04-01" @default.
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- W2022385542 title "Structural characterization of tripodal phosphine complexes of transition metals. Examples of chair and twisted-boat conformations in six-membered chelate rings" @default.
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- W2022385542 doi "https://doi.org/10.1016/0022-328x(90)87302-t" @default.
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