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- W2022386725 startingPage "2614" @default.
- W2022386725 abstract "The alkaline hydrolysis of bis(nitromethyl)prehnitene (1) with aqueous sodium hydroxide gave almost quantitatively disodium tetramethylphthalate (11). Under milder conditions the sodium salts of tetramethylphthalimide (8), N-hydroxytetramethylphthalimide (10), and 2-hydroxy-3-hydroxyimino-4,5,6,7-tetramethylphthalimide (9) were fo were formed, probably as intermediate products of the above reaction. But, pentamethylphenylnitromethane (14) and bis(nitromethyl)isodurene (15) were not hydrolyzed in an aqueous base. From the above results, it is recognized that the sodium nitronate from 1 is unstable in a different way from general nitronates such as the sodium salt of 14 or 15. It appears that the instability of 1 arises from the two adjacent nitromethyl groups on the benzene ring." @default.
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- W2022386725 date "1976-09-01" @default.
- W2022386725 modified "2023-10-18" @default.
- W2022386725 title "The Preparation of Tetramethylphthalic Anhydride" @default.
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